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Mohrig Techniques in Organic Chemistry PDF Form

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Professor Dave here, let’s talk about recrystallization. After learning a variety of separation techniques, we will need to look at just one technique for the purification of solids. Sometimes a chemical reaction will occur such that a solid preciptate will form, which we can then filter out of solution. But it is inevitable that this solid will contain impurities. When the lattice structure is forming during the precipitation, ions and other particles that do not belong in the lattice will get trapped inside and disrupt the pattern of the lattice. There is a solution to this problem, and it is called recrystallization, so let’s see how that works now. Let’s say we have our impure solid that we wish to recrystallize. The way this works is that we will choose a very particular solvent in which to dissolve this solid. The solid must have a very low solubility in this solvent at room temperature, but a very high solubility in this solvent at very high temperatures, which makes sense

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