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5890  Form

5890 Form

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Video instructions and help with filling out and completing 5890 Form

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this video covers the standard operating procedure for our hewlett packard 5890 5971 gas chromatograph mass spectrometer the large box in the center is an oven and contains the capillary column for our separation the detector is the small unit at the far left and contains a quadrupole mass spectrometer capable of scanning up to 600 atomic mass units the helium carrier gas is supplied from a tank behind the instrument please note the pressure on the tank as indicated at the gauge on the right the helium should be left on at all times if this drops below 200 pounds per square inch please notify your instructor the heart of the gas chromatograph is the separation column modern analytical columns are made from fused silica capillaries typically these columns are from 25 to 50 meters long it may seem surprising that glass can be coiled like a wire glass is actually quite tough and flexible if one can prevent scratches on the surface this capillary appears brown because it has a tough polyem

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